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CRYSTAL-STRUCTURE OF AN ORTHORHOMBIC FORM OF ADENOSINE-5'-MONOPHOSPHATE

NEIDLE, S; KUHLBRANDT, W; ACHARI, A; (1976) CRYSTAL-STRUCTURE OF AN ORTHORHOMBIC FORM OF ADENOSINE-5'-MONOPHOSPHATE. ACTA CRYSTALLOGRAPHICA SECTION B-STRUCTURAL SCIENCE , 32 (Part 6) 1850 - 1855. 10.1107/S0567740876006511. Green open access

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Abstract

Adenosine-Y-phosphate monohydrate was crystallized in the orthorhombic space group P212121, with a=22"997 (2), b=9.406 (1), c=6.599 (1)A,, Z=4. The structure was solved by direct methods and refined to a final Rw of 0.0639 for 1320 significant reflexions measured on an automatic diffractometer. The conformation of the molecule differs significantly from that previously reported for the monoclinic monohydrate [Kraut & Jensen, Acta Cryst. (1963), 16, 79-88]. The sugar conformation, for example, is here C(2)'-endo, and the glycosidic torsion angle has altered by almost 50 °.

Type: Article
Title: CRYSTAL-STRUCTURE OF AN ORTHORHOMBIC FORM OF ADENOSINE-5'-MONOPHOSPHATE
Open access status: An open access version is available from UCL Discovery
DOI: 10.1107/S0567740876006511
Publisher version: http://scripts.iucr.org/cgi-bin/paper?S05677408760...
Language: English
Additional information: Copyright © International Union of Crystallography
UCL classification: UCL
UCL > Provost and Vice Provost Offices
UCL > Provost and Vice Provost Offices > School of Life and Medical Sciences
UCL > Provost and Vice Provost Offices > School of Life and Medical Sciences > Faculty of Life Sciences
UCL > Provost and Vice Provost Offices > School of Life and Medical Sciences > Faculty of Life Sciences > UCL School of Pharmacy
URI: https://discovery.ucl.ac.uk/id/eprint/1367880
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