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4‐cyano‐2‐methoxybenzenesulfonyl chloride

Bayle, ED; Igoe, N; Fish, PV; (2018) 4‐cyano‐2‐methoxybenzenesulfonyl chloride. Organic Syntheses , 94 10.1002/0471264229.os094.15. Green open access

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Abstract

Procedures yielding O‐(4‐cyano‐2‐methoxyphenyl) dimethylcarbamothioate (1) as white crystals, S‐(4‐cyano‐2‐methoxy‐phenyl)dimethylcarbamothioate (2) as a pure product, 4‐mercapto‐3‐methoxybenzonitrile (3) (14.4 g, 90%) as a slightly pungent white solid, and 4‐cyano‐2‐methoxybenzenesulfonyl chloride (4) as a yellow solid are presented. The chapter concludes with a discussion on sulfonamide functional group and related syntheses.

Type: Article
Title: 4‐cyano‐2‐methoxybenzenesulfonyl chloride
Open access status: An open access version is available from UCL Discovery
DOI: 10.1002/0471264229.os094.15
Publisher version: http://doi.org/10.1002/0471264229.os094.15
Additional information: This version is the author accepted manuscript. For information on re-use, please refer to the publisher’s terms and conditions.
Keywords: 4‐cyano‐2‐methoxybenzenesulfonyl chloride, dimethylcarbamothioate, dimethylthiocarbamoyl chloride, toluene, aqueous hydrochloric acid
UCL classification: UCL
UCL > Provost and Vice Provost Offices
UCL > Provost and Vice Provost Offices > School of Life and Medical Sciences
UCL > Provost and Vice Provost Offices > School of Life and Medical Sciences > Faculty of Brain Sciences
UCL > Provost and Vice Provost Offices > School of Life and Medical Sciences > Faculty of Brain Sciences > UCL Queen Square Institute of Neurology
UCL > Provost and Vice Provost Offices > School of Life and Medical Sciences > Faculty of Brain Sciences > UCL Queen Square Institute of Neurology > Department of Neuromuscular Diseases
URI: https://discovery.ucl.ac.uk/id/eprint/10060471
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