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High-resolution neutron-diffraction measurements to 8 kbar

Bull, CL; Fortes, AD; Ridley, CJ; Wood, IG; Dobson, DP; Funnell, NP; Gibbs, AS; ... Knight, KS; + view all (2017) High-resolution neutron-diffraction measurements to 8 kbar. High Pressure Research , 37 (4) pp. 486-494. 10.1080/08957959.2017.1386183. Green open access

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Abstract

We describe the capability to measure high-resolution neutron powder diffraction data to a pressure of at least 8 kbar. We have used the HRPD instrument at the ISIS neutron source and a piston-cylinder design of pressure cell machined from a null-scattering titanium zirconium alloy. Data were collected under hydrostatic conditions from an elpasolite perovskite La(Formula presented.)NiMnO(Formula presented.); by virtue of a thinner cell wall on the incident-beam side of the cell, it was possible to obtain data in the instrument's highest resolution back-scattering detector banks up to a maximum pressure of 8.5 kbar.

Type: Article
Title: High-resolution neutron-diffraction measurements to 8 kbar
Open access status: An open access version is available from UCL Discovery
DOI: 10.1080/08957959.2017.1386183
Publisher version: https://doi.org/10.1080/08957959.2017.1386183
Language: English
Additional information: This version is the author accepted manuscript. For information on re-use, please refer to the publisher’s terms and conditions.
Keywords: Neutron diffraction, high pressure, perovskite, high resolution
UCL classification: UCL
UCL > Provost and Vice Provost Offices > UCL BEAMS
UCL > Provost and Vice Provost Offices > UCL BEAMS > Faculty of Maths and Physical Sciences
UCL > Provost and Vice Provost Offices > UCL BEAMS > Faculty of Maths and Physical Sciences > Dept of Earth Sciences
URI: https://discovery.ucl.ac.uk/id/eprint/10026170
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