TY - JOUR PB - The Royal Society of Chemistry N2 - Catastrophic failure of lithium-ion batteries occurs across multiple length scales and over very short time periods. A combination of high-speed operando tomography, thermal imaging and electrochemical measurements is used to probe the degradation mechanisms leading up to overcharge-induced thermal runaway of a LiCoO2 pouch cell, through its interrelated dynamic structural, thermal and electrical responses. Failure mechanisms across multiple length scales are explored using a post-mortem multi-scale tomography approach, revealing significant morphological and phase changes in the LiCoO2 electrode microstructure and location dependent degradation. This combined operando and multi-scale X-ray computed tomography (CT) technique is demonstrated as a comprehensive approach to understanding battery degradation and failure. ID - discovery1514067 AV - public Y1 - 2016/12/07/ EP - 30919 TI - Investigating lithium-ion battery materials during overcharge-induced thermal runaway: an operando and multi-scale X-ray CT study UR - http://dx.doi.org/10.1039/C6CP04251A SN - 1463-9076 A1 - Finegan, DP A1 - Scheel, M A1 - Robinson, JB A1 - Tjaden, B A1 - Di Michiel, M A1 - Hinds, G A1 - Brett, DJL A1 - Shearing, PR JF - Physical Chemistry Chemical Physics VL - 18 SP - 30912 IS - 45 N1 - This article is licensed under a Creative Commons Attribution 3.0 Unported Licence (http://creativecommons.org/licenses/by/3.0/). ER -