eprintid: 1487098 rev_number: 26 eprint_status: archive userid: 608 dir: disk0/01/48/70/98 datestamp: 2016-05-01 12:09:42 lastmod: 2021-09-19 23:44:35 status_changed: 2016-08-11 16:48:02 type: article metadata_visibility: show creators_name: Huang, X creators_name: Yang, W creators_name: Harder, R creators_name: Sun, Y creators_name: Lu, M creators_name: Chu, YS creators_name: Robinson, IK creators_name: Mao, HK title: Deformation Twinning of a Silver Nanocrystal under High Pressure ispublished: pub divisions: UCL divisions: B04 divisions: C06 divisions: F64 keywords: Nanocrystal, X-ray imaging, coherent diffractive imaging, deformation twinning note: This document is the Accepted Manuscript version of a Published Work that appeared in final form in Nano Letters, copyright © American Chemical Society after peer review and technical editing by the publisher. To access the final edited and published work see [insert ACS Articles on Request author-directed link to Published Work, see: http://dx.doi.org/10.1021/acs.nanolett.5b03568. abstract: Within a high-pressure environment, crystal deformation is controlled by complex processes such as dislocation motion, twinning, and phase transitions, which change materials' microscopic morphology and alter their properties. Understanding a crystal's response to external stress provides a unique opportunity for rational tailoring of its functionalities. It is very challenging to track the strain evolution and physical deformation from a single nanoscale crystal under high-pressure stress. Here, we report an in situ three-dimensional mapping of morphology and strain evolutions in a single-crystal silver nanocube within a high-pressure environment using the Bragg Coherent Diffractive Imaging (CDI) method. We observed a continuous lattice distortion, followed by a deformation twining process at a constant pressure. The ability to visualize stress-introduced deformation of nanocrystals with high spatial resolution and prominent strain sensitivity provides an important route for interpreting and engineering novel properties of nanomaterials. date: 2015-11-11 date_type: published official_url: http://dx.doi.org/10.1021/acs.nanolett.5b03568 oa_status: green full_text_type: other language: eng primo: open primo_central: open_green article_type_text: Journal Article verified: verified_manual elements_id: 1093720 doi: 10.1021/acs.nanolett.5b03568 lyricists_name: Robinson, Ian lyricists_id: IKROB22 full_text_status: public publication: Nano Letters volume: 15 number: 11 pagerange: 7644-7649 event_location: United States issn: 1530-6992 citation: Huang, X; Yang, W; Harder, R; Sun, Y; Lu, M; Chu, YS; Robinson, IK; Huang, X; Yang, W; Harder, R; Sun, Y; Lu, M; Chu, YS; Robinson, IK; Mao, HK; - view fewer <#> (2015) Deformation Twinning of a Silver Nanocrystal under High Pressure. Nano Letters , 15 (11) pp. 7644-7649. 10.1021/acs.nanolett.5b03568 <https://doi.org/10.1021/acs.nanolett.5b03568>. Green open access document_url: https://discovery.ucl.ac.uk/id/eprint/1487098/1/Robinson_Xiaojing_NanoLett_AnvilAg_v4.pdf