eprintid: 1452708 rev_number: 39 eprint_status: archive userid: 608 dir: disk0/01/45/27/08 datestamp: 2014-10-26 20:21:00 lastmod: 2021-09-19 23:49:44 status_changed: 2014-10-26 20:21:00 type: article metadata_visibility: show item_issues_count: 0 creators_name: Robinson, JB creators_name: Brown, LD creators_name: Jervis, R creators_name: Taiwo, OO creators_name: Millichamp, J creators_name: Mason, TJ creators_name: Neville, TP creators_name: Eastwood, DS creators_name: Reinhard, C creators_name: Lee, PD creators_name: Brett, DJ creators_name: Shearing, PR title: A novel high-temperature furnace for combined in situ synchrotron X-ray diffraction and infrared thermal imaging to investigate the effects of thermal gradients upon the structure of ceramic materials. ispublished: pub divisions: UCL divisions: B04 divisions: C05 divisions: F43 divisions: F45 keywords: X-ray diffraction, composite materials, infrared imaging, solid oxide fuel cell, stress analysis, thermal imaging note: This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited. abstract: A new technique combining in situ X-ray diffraction using synchrotron radiation and infrared thermal imaging is reported. The technique enables the application, generation and measurement of significant thermal gradients, and furthermore allows the direct spatial correlation of thermal and crystallographic measurements. The design and implementation of a novel furnace enabling the simultaneous thermal and X-ray measurements is described. The technique is expected to have wide applicability in material science and engineering; here it has been applied to the study of solid oxide fuel cells at high temperature. date: 2014-09 official_url: http://dx.doi.org/10.1107/S1600577514014209 vfaculties: VENG oa_status: green full_text_type: pub language: eng primo: open primo_central: open_green article_type_text: Journal Article, Research Support, Non-U.S. Gov't verified: verified_manual elements_source: PubMed elements_id: 987058 doi: 10.1107/S1600577514014209 pii: S1600577514014209 lyricists_name: Brett, Daniel lyricists_name: Jervis, John lyricists_name: Lee, Peter lyricists_name: Mason, Thomas lyricists_name: Millichamp, Jason lyricists_name: Neville, Tobias lyricists_name: Robinson, James lyricists_name: Shearing, Paul lyricists_id: DBRET49 lyricists_id: JRJER29 lyricists_id: PLEEX57 lyricists_id: TMASO26 lyricists_id: JMILL72 lyricists_id: TNEVI40 lyricists_id: ROBIN60 lyricists_id: PSHEA33 full_text_status: public publication: J Synchrotron Radiat volume: 21 number: 5 pagerange: 1134 - 1139 event_location: United States citation: Robinson, JB; Brown, LD; Jervis, R; Taiwo, OO; Millichamp, J; Mason, TJ; Neville, TP; ... Shearing, PR; + view all <#> Robinson, JB; Brown, LD; Jervis, R; Taiwo, OO; Millichamp, J; Mason, TJ; Neville, TP; Eastwood, DS; Reinhard, C; Lee, PD; Brett, DJ; Shearing, PR; - view fewer <#> (2014) A novel high-temperature furnace for combined in situ synchrotron X-ray diffraction and infrared thermal imaging to investigate the effects of thermal gradients upon the structure of ceramic materials. J Synchrotron Radiat , 21 (5) 1134 - 1139. 10.1107/S1600577514014209 <https://doi.org/10.1107/S1600577514014209>. Green open access document_url: https://discovery.ucl.ac.uk/id/eprint/1452708/1/pp5048.pdf