eprintid: 1424789 rev_number: 30 eprint_status: archive userid: 608 dir: disk0/01/42/47/89 datestamp: 2014-03-25 22:25:14 lastmod: 2021-10-04 01:43:31 status_changed: 2014-03-25 22:25:14 type: article metadata_visibility: show item_issues_count: 0 creators_name: Kubas, A creators_name: De Sancho, D creators_name: Best, RB creators_name: Blumberger, J title: Aerobic Damage to [FeFe]-Hydrogenases: Activation Barriers for the Chemical Attachment of O2. ispublished: pub divisions: UCL divisions: B04 divisions: C06 divisions: F60 keywords: [FeFe]-hydrogenases, ab initio calculations, electron transfer, iron-sulfur clusters, oxygen activation note: © 2014 The Authors. Published by Wiley-VCH Verlag GmbH & Co. KGaA. This is an open access article under the terms of the Creative Commons Attribution License, which permits use, distribution and reproduction in any medium, provided the original work is properly cited. abstract: [FeFe]-hydrogenases are the best natural hydrogen-producing enzymes but their biotechnological exploitation is hampered by their extreme oxygen sensitivity. The free energy profile for the chemical attachment of O2 to the enzyme active site was investigated by using a range-separated density functional re-parametrized to reproduce high-level ab initio data. An activation free-energy barrier of 13 kcal mol(-1) was obtained for chemical bond formation between the di-iron active site and O2 , a value in good agreement with experimental inactivation rates. The oxygen binding can be viewed as an inner-sphere electron-transfer process that is strongly influenced by Coulombic interactions with the proximal cubane cluster and the protein environment. The implications of these results for future mutation studies with the aim of increasing the oxygen tolerance of this enzyme are discussed. date: 2014-04-14 official_url: http://dx.doi.org/10.1002/anie.201400534 vfaculties: VMPS oa_status: green full_text_type: pub primo: open primo_central: open_green article_type_text: JOURNAL ARTICLE verified: verified_manual elements_source: PubMed elements_id: 938503 doi: 10.1002/anie.201400534 language_elements: ENG lyricists_name: Blumberger, Jochen lyricists_name: Kubas, Adam lyricists_id: JBLUM96 lyricists_id: AKUBA18 full_text_status: public publication: Angew Chem Int Ed Engl volume: 53 number: 16 pagerange: 4081-4084 citation: Kubas, A; De Sancho, D; Best, RB; Blumberger, J; (2014) Aerobic Damage to [FeFe]-Hydrogenases: Activation Barriers for the Chemical Attachment of O2. Angew Chem Int Ed Engl , 53 (16) pp. 4081-4084. 10.1002/anie.201400534 <https://doi.org/10.1002/anie.201400534>. Green open access document_url: https://discovery.ucl.ac.uk/id/eprint/1424789/1/4081_ftp.pdf