eprintid: 10205497 rev_number: 7 eprint_status: archive userid: 699 dir: disk0/10/20/54/97 datestamp: 2025-03-03 16:12:47 lastmod: 2025-03-03 16:12:47 status_changed: 2025-03-03 16:12:47 type: article metadata_visibility: show sword_depositor: 699 creators_name: Cheng, R creators_name: He, X creators_name: Ran, B creators_name: Li, H creators_name: Tang, W creators_name: Sun, F creators_name: Li, K creators_name: Shao, X creators_name: Chen, H creators_name: Fu, C title: High-entropy optimizing d-orbital electronic configuration of metal organic framework for high-current-density anion exchange membrane water electrolysis ispublished: pub divisions: UCL divisions: B04 divisions: C06 divisions: F43 divisions: F56 keywords: High-entropy; metal organic framework; d-orbital; large current density; overall water splitting note: This version is the author accepted manuscript. For information on re-use, please refer to the publisher’s terms and conditions. abstract: Water electrolysis provides a promising way for hydrogen production through renewable power sources. The exploration of non-precious metal-based electrocatalysts capable of sustaining high current densities for water electrocatalysis is of critical importance. Herein, we develop a high-entropy Mil53 metal organic framework (denoted as Mil53-HE) bifunctional electrocatalyst with improved performance for overall water splitting at large current densities. The improved activity and stability of Mil53-HE for water electrolysis stem from the optimized electronic configurations of d-orbitals in the metal centers, as the overall d-band center (E̅d) is upshifted and the total number of d-orbital electrons in the supercell (∑Nd) is decreased of Mil53-HE. Therefore, the reduced reaction energy barriers and enriched unpaired d-electrons promote both the oxygen evolution reaction (OER) and hydrogen evolution reaction (HER). As a result, the HER and OER activities of Mil53-HE surpass those of their benchmarks Pt/C and RuO2, respectively. Meanwhile, the HER and OER mechanisms on Mil53-HE are revealed by in-situ characterizations and theoretical calculations. Furthermore, the anion exchange membrane water electrolysis cell with Mil53-HE can stably operate at large current densities with small voltages (1.9 V at 0.52 A cm−2 and 2.1 V at 1.48 A cm−2), demonstrating good feasibility for practical application. date: 2025-02 date_type: published publisher: ELSEVIER official_url: https://doi.org/10.1016/j.nanoen.2024.110529 full_text_type: other language: eng verified: verified_manual elements_id: 2343288 doi: 10.1016/j.nanoen.2024.110529 lyricists_name: Li, Kaiqi lyricists_name: Li, Huanxin lyricists_id: KLIDX18 lyricists_id: HLIPX63 actors_name: Li, Huanxin actors_id: HLIPX63 actors_role: owner funding_acknowledgements: 22ZR1429700 [Natural Science Foundation of Shanghai]; 52274302 [National Natural Science Foundation of China] full_text_status: restricted publication: Nano Energy volume: 134 article_number: 110529 pages: 13 issn: 2211-2855 citation: Cheng, R; He, X; Ran, B; Li, H; Tang, W; Sun, F; Li, K; ... Fu, C; + view all <#> Cheng, R; He, X; Ran, B; Li, H; Tang, W; Sun, F; Li, K; Shao, X; Chen, H; Fu, C; - view fewer <#> (2025) High-entropy optimizing d-orbital electronic configuration of metal organic framework for high-current-density anion exchange membrane water electrolysis. Nano Energy , 134 , Article 110529. 10.1016/j.nanoen.2024.110529 <https://doi.org/10.1016/j.nanoen.2024.110529>. document_url: https://discovery.ucl.ac.uk/id/eprint/10205497/1/NE_final.pdf