TY - JOUR N2 - Direct methane conversion to high-value chemicals under mild conditions is attractive yet challenging due to the inertness of methane and the high reactivity of valuable products. This work presents an efficient and selective strategy to achieve direct methane conversion through the oxidative coupling of methane over a visible-responsive Au-loaded CeO2 by photon-phonon co-driven catalysis. A record-high ethane yield of 755??mol h?1 (15,100??mol g?1 h?1) and selectivity of 93% are achieved under optimised reaction conditions, corresponding to an apparent quantum efficiency of 12% at 365?nm. Moreover, the high activity of the photocatalyst can be maintained for at least 120?h without noticeable decay. The pre-treatment of the catalyst at relatively high temperatures introduces oxygen vacancies, which improves oxygen adsorption and activation. Furthermore, Au, serving as a hole acceptor, facilitates charge separation, inhibits overoxidation and promotes the C-C coupling reaction. All these enhance photon efficiency and product yield. VL - 15 PB - Springer Science and Business Media LLC Y1 - 2024/08/30/ A1 - Wang, Chao A1 - Xu, Youxun A1 - Xiong, Lunqiao A1 - Li, Xiyi A1 - Chen, Enqi A1 - Miao, Tina Jingyan A1 - Zhang, Tianyu A1 - Lan, Yang A1 - Tang, Junwang ID - discovery10196574 SN - 2041-1723 N1 - © The Author(s), 2024. This is an Open Access article distributed under the terms of the Creative Commons Attribution Licence (CC BY 4.0), which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is properly cited. https://creativecommons.org/licenses/by/4.0/ JF - Nature Communications AV - public UR - https://doi.org/10.1038/s41467-024-51690-2 KW - Heterogeneous catalysis KW - Photocatalysis TI - Selective oxidation of methane to C2+ products over Au-CeO2 by photon-phonon co-driven catalysis. ER -