eprintid: 10149215 rev_number: 8 eprint_status: archive userid: 699 dir: disk0/10/14/92/15 datestamp: 2022-05-25 11:51:58 lastmod: 2023-05-11 06:10:10 status_changed: 2022-05-25 11:51:58 type: article metadata_visibility: show sword_depositor: 699 creators_name: Singla, Pankaj creators_name: Garg, Saweta creators_name: Kaur, Sarbjeet creators_name: Kaur, Navreet creators_name: Kaur, Navalpreet creators_name: Aswal, Vinod K creators_name: Velliou, Eirini creators_name: Kaur, Harpreet creators_name: Peeters, Marloes creators_name: Kumar Mahajan, Rakesh title: Unusual solubilization capacity of hydrophobic drug olanzapine in polysorbate micelles for improved sustained drug release ispublished: pub divisions: C10 divisions: G88 divisions: B02 divisions: UCL divisions: D16 keywords: Olanzapine, Hydrophobic drug, Loading capacity, Polysorbates, Oral delivery, Small angle neutron scattering note: This version is the author accepted manuscript. For information on re-use, please refer to the publisher’s terms and conditions. abstract: Polysorbates and Pluronic polymers are straightforward to use to improve the performance of hydrophobic molecules, however, colloidal systems of these polymers are not fully understood and loading of drug molecules in these Polysorbate micelles rely on a plethora of factors. Thus, it is a laborious task to select the optimal Polysorbate as a drug delivery vehicle. To pave the way for use of Polysorbates, three Polysorbates with different hydrophobicity were selected for oral delivery of the hydrophobic drug Olanzapine (OLZ). At higher concentration, Polysorbate T20 with low hydrophobicity accommodated a higher amount of OLZ than other Polysorbates T40 and T60 with higher hydrophobicity. The effect of mixed micelles of Pluronic P84 and Polysorbate (T20, T40, T60) on solubilization of OLZ was also studied at different concentration ratios and the higher OLZ solubilization was found to be in T20:P84 mixed micelles at 3:2 %w/v concentration ratio. Stronger interactions between OLZ and T20 were noticed with isothermal titration calorimetry (ITC), resulting in the higher OLZ solubilization in these micelles. Dynamic light scattering (DLS) and small angle neutron scattering (SANS) measurements revealed that mixed micelles of Polysorbates are greater in sizes than pure polysorbate micelles and the size decreased after loading of OLZ. Furthermore, SANS measurements suggested that decrease in the aggregation number after OLZ loading promoted the loading capacity of the Polysorbate micelle. Polysorbates micelles exhibited the sustained release behavior in biological relevant media, examined with in vitro dialysis release method. Therefore, it is believed that the finding of this work could be useful in the oral delivery formulations in which Polysorbates and Pluronics are primarily used. date: 2022-08 date_type: published publisher: Elsevier BV official_url: https://doi.org/10.1016/j.molliq.2022.119256 oa_status: green full_text_type: other language: eng primo: open primo_central: open_green verified: verified_manual elements_id: 1958199 doi: 10.1016/j.molliq.2022.119256 lyricists_name: Velliou, Eirini lyricists_id: EVELL97 actors_name: Velliou, Eirini actors_name: Allington-Smith, Dominic actors_id: EVELL97 actors_id: DAALL44 actors_role: owner actors_role: impersonator full_text_status: public publication: Journal of Molecular Liquids volume: 359 article_number: 119256 citation: Singla, Pankaj; Garg, Saweta; Kaur, Sarbjeet; Kaur, Navreet; Kaur, Navalpreet; Aswal, Vinod K; Velliou, Eirini; ... Kumar Mahajan, Rakesh; + view all <#> Singla, Pankaj; Garg, Saweta; Kaur, Sarbjeet; Kaur, Navreet; Kaur, Navalpreet; Aswal, Vinod K; Velliou, Eirini; Kaur, Harpreet; Peeters, Marloes; Kumar Mahajan, Rakesh; - view fewer <#> (2022) Unusual solubilization capacity of hydrophobic drug olanzapine in polysorbate micelles for improved sustained drug release. Journal of Molecular Liquids , 359 , Article 119256. 10.1016/j.molliq.2022.119256 <https://doi.org/10.1016/j.molliq.2022.119256>. Green open access document_url: https://discovery.ucl.ac.uk/id/eprint/10149215/1/Velliou_Revised%20Manuscript%20unmarked10.pdf