TY - JOUR A1 - Xie, J A1 - Shevlin, SA A1 - Ruan, Q A1 - Moniz, SJA A1 - Liu, Y A1 - Liu, X A1 - Li, Y A1 - Lau, CC A1 - Guo, ZX A1 - Tang, J JF - Energy and Environmental Science UR - http://dx.doi.org/10.1039/c7ee02981k SN - 1754-5706 IS - 6 N1 - This article is licensed under a Creative Commons Attribution 3.0 Unported Licence. (https://creativecommons.org/licenses/by/3.0/) SP - 1617 VL - 11 KW - Science & Technology KW - Physical Sciences KW - Technology KW - Life Sciences & Biomedicine KW - Chemistry KW - Multidisciplinary KW - Energy & Fuels KW - Engineering KW - Chemical KW - Environmental Sciences KW - Chemistry KW - Engineering KW - Environmental Sciences & Ecology KW - GRAPHITIC CARBON NITRIDE KW - PHOTOCATALYTIC HYDROGEN-PRODUCTION KW - PHOTOELECTROCHEMICAL DEVICES KW - POLYMERIC PHOTOCATALYST KW - CONJUGATED POLYMERS KW - ORGANIC FRAMEWORK KW - EVOLUTION KW - GENERATION KW - DESIGN KW - ENERGY PB - ROYAL SOC CHEMISTRY N2 - Water oxidation is a rate-determining step in solar driven H2 fuel synthesis and is technically challenging to promote. Despite decades of effort, only a few inorganic catalysts are effective and even fewer are effective under visible light. Recently, attention has been paid to synthetic semiconducting polymers, mainly on graphitic C3N4, with encouraging hydrogen evolution performance but lower activity for water oxidation. Here, a highly ordered covalent triazine-based framework, CTF-1 (C8N2H4), is synthesised by a very mild microwave-assisted polymerisation approach. It demonstrates extremely high activity for oxygen evolution under visible light irradiation, leading to an apparent quantum efficiency (AQE) of nearly 4% at 420 nm. Furthermore, the polymer can also efficiently evolve H2 from water. A high AQE of 6% at 420 nm for H2 production has also been achieved. The polymer holds great potential for overall water splitting. This exceptional performance is attributed to its well-defined and ordered structure, low carbonisation, and superior band positions. ID - discovery10052903 AV - public Y1 - 2018/06/01/ EP - 1624 TI - Efficient visible light-driven water oxidation and proton reduction by an ordered covalent triazine-based framework ER -