TY - JOUR JF - ChemistrySelect AV - public KW - Science & Technology KW - Physical Sciences KW - Chemistry KW - Multidisciplinary KW - Chemistry KW - Continuous hydrothermal flow synthesis KW - MnO2 KW - doping KW - oxygen reduction KW - oxygen evolution KW - Zn-air batteries KW - ZINC-AIR BATTERIES KW - LITHIUM-ION BATTERIES KW - HIGH-PERFORMANCE KW - TEMPERATURE SYNTHESIS KW - NEGATIVE ELECTRODES KW - MANGANESE-DIOXIDE KW - WATER OXIDATION KW - ALKALINE MEDIA KW - OXIDE KW - ELECTROCATALYSTS IS - 9 SP - 2613 SN - 2365-6549 A1 - Lubke, M A1 - Sumboja, A A1 - McCafferty, L A1 - Armer, CF A1 - Handoko, AD A1 - Du, Y A1 - McColl, K A1 - Cora, F A1 - Brett, D A1 - Liu, Z A1 - Darr, JA UR - https://doi.org/10.1002/slct.201702514 VL - 3 N2 - Nano?sized ??MnO2 nanorods doped with Co or Ru were directly synthesized using a continuous hydrothermal synthesis process (production rate 10?g h?1) and investigated as relatively inexpensive (due to the small Ru content) bifunctional catalysts for both the Oxygen Reduction Reaction (ORR) and Oxygen Evolution Reaction (OER). The materials were extensively characterized using a range of analytical methods; these including Extended X?Ray Absorption Fine Structure (EXAFS) spectroscopy measurements, which was accompanied by density functional theory studies, in order to elucidate the role of dopants in ??MnO2 structure. Electrochemical ORR and OER investigations of the as?prepared doped ??MnO2 nanomaterials were compared to more expensive Pt/C or RuO2 catalysts. The doped manganese oxide nanomaterials were used as bifunctional catalysts in the positive electrode of zinc air batteries (with oversized zinc metal negative electrode and limited density of discharge window) and displayed excellent performance (the overpotential was 0.77 and 0.68?V for ??MnO2 modified with 7.6 at% Co and 9.4 at% Ru, respectively). Overall, as a result of doping, this study achieved improved bifunctional catalytic activities of metal oxide catalysts, which was comparable to more expensive alternatives. EP - 2622 ID - discovery10049213 PB - WILEY-V C H VERLAG GMBH N1 - This version is the author accepted manuscript. For information on re-use, please refer to the publisher?s terms and conditions. TI - Transition-Metal-Doped alpha-MnO2 Nanorods as Bifunctional Catalysts for Efficient Oxygen Reduction and Evolution Reactions Y1 - 2018/03/05/ ER -