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Solid-phase intermolecular radical reactions 2: Synthesis of C-glycopeptide mimetics via a novel acrylate acceptor

Caddick, S; Hamza, D; Wadman, SN; Wilden, JD; (2002) Solid-phase intermolecular radical reactions 2: Synthesis of C-glycopeptide mimetics via a novel acrylate acceptor. ORG LETT , 4 (10) 1775 - 1777. 10.1021/ol025846h.

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Abstract

[GRAPHICS]A novel tetrafluorophenol-linked acrylate is reported as an activated acceptor for intermolecular radical reactions. Addition of alkyl radicals led to pure products in good yields. We include here the first syntheses of C1- and C6-linked glycosides using a solid-phase radical methodology.

Type: Article
Title: Solid-phase intermolecular radical reactions 2: Synthesis of C-glycopeptide mimetics via a novel acrylate acceptor
DOI: 10.1021/ol025846h
Keywords: ALKENES, SUPPORT
UCL classification: UCL > School of BEAMS > Faculty of Maths and Physical Sciences > Chemistry
UCL > VP Enterprise
URI: http://discovery.ucl.ac.uk/id/eprint/9454
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