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Synthesis and characterization of (arene)ruthenium(II)poly(pyrazolyl)borate and poly(pyrazolyl)methane complexes

Bhambri, S; Tocher, DA; (1996) Synthesis and characterization of (arene)ruthenium(II)poly(pyrazolyl)borate and poly(pyrazolyl)methane complexes. POLYHEDRON , 15 (16) 2763 - 2770.

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Abstract

A range of compounds of the formulae [Ru(eta(6)-arene) (HBPz(3))][PF6] and [Ru(eta(6)- arene) (HCPz(3))][PF6](2) (Pz = pyrazolyl) has been prepared by a modification of the literature method. These compounds have all been characterized by H-1 and C-13 NMR spectroscopy and the X-ray crystal structures of [Ru(eta(6)-p-cymene) (HBPz(3))][PF6] and [RU(eta(6)-p-cymene)(HCPz(3))] [PF6](2) have been determined. The previously elusive compound [Ru(eta(6)-C6H6) (HB{3,5-Me(2)Pz}(3))][PF6] was observed for the first time. Copyright (C) 1996 Elsevier Science Ltd

Type:Article
Title:Synthesis and characterization of (arene)ruthenium(II)poly(pyrazolyl)borate and poly(pyrazolyl)methane complexes
Keywords:CRYSTAL-STRUCTURE, LIGANDS, RUTHENIUM, NUCLEOPHILES
UCL classification:UCL > School of BEAMS > Faculty of Maths and Physical Sciences > Chemistry

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