Sankar, G and Thomas, JM and Rey, F and Greaves, GN (1995) Probing the onset of crystallization of a microporous catalyst by combined X-ray absorption spectroscopy and X-ray diffraction. J CHEM SOC CHEM COMM (24) 2549 - 2550.
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Abstract
The power of a new variant of the in situ combined XRA-XRD experiment (see ref. 12) is illustrated by tracking the inner shell environment and bonding of a Co-II ion as it changes, in the gel just prior to crystallisation, from octahedral to tetrahedral coordination, the state in which it finally appears in the microporous catalyst CoAIPO-5: the technique is widely applicable.
| Type: | Article |
|---|---|
| Title: | Probing the onset of crystallization of a microporous catalyst by combined X-ray absorption spectroscopy and X-ray diffraction |
| Keywords: | IN-SITU, SPECTRA, XRD |
| UCL classification: | UCL > School of BEAMS > Faculty of Maths and Physical Sciences > Chemistry |
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