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Probing the onset of crystallization of a microporous catalyst by combined X-ray absorption spectroscopy and X-ray diffraction

Sankar, G; Thomas, JM; Rey, F; Greaves, GN; (1995) Probing the onset of crystallization of a microporous catalyst by combined X-ray absorption spectroscopy and X-ray diffraction. J CHEM SOC CHEM COMM (24) 2549 - 2550.

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Abstract

The power of a new variant of the in situ combined XRA-XRD experiment (see ref. 12) is illustrated by tracking the inner shell environment and bonding of a Co-II ion as it changes, in the gel just prior to crystallisation, from octahedral to tetrahedral coordination, the state in which it finally appears in the microporous catalyst CoAIPO-5: the technique is widely applicable.

Type:Article
Title:Probing the onset of crystallization of a microporous catalyst by combined X-ray absorption spectroscopy and X-ray diffraction
Keywords:IN-SITU, SPECTRA, XRD
UCL classification:UCL > School of BEAMS > Faculty of Maths and Physical Sciences > Chemistry

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