ALIEV, AE; HARRIS, KDM; APPERLEY, DC; (1993) HIGH-RESOLUTION SOLID-STATE C-13 AND SI-29 NMR INVESTIGATIONS OF THE DYNAMIC PROPERTIES OF TETRAKIS(TRIMETHYLSILYL)SILANE. J CHEM SOC CHEM COMM (3) 251 - 253.
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High-resolution solid-state C-13 and Si-29 NMR spectroscopy have been used to investigate the dynamic properties of tetrakis(trimethylsilyl)silane (TTMSS) as a function of temperature; from the temperature dependence of the spectra, it is clear that TTMSS is not useful as a chemical shift reference material below ca. 238 K, but the spectral changes associated with the phase transition at this temperature nevertheless provide a precise method for controlling temperature calibration in low-temperature solid-state C-13 NMR studies.
|Title:||HIGH-RESOLUTION SOLID-STATE C-13 AND SI-29 NMR INVESTIGATIONS OF THE DYNAMIC PROPERTIES OF TETRAKIS(TRIMETHYLSILYL)SILANE|
|UCL classification:||UCL > School of BEAMS > Faculty of Maths and Physical Sciences > Chemistry|
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