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STRUCTURAL AND DYNAMIC PROPERTIES OF THE C-60/N-PENTANE INCLUSION COMPOUND - SOLID-STATE C-13 NUCLEAR-MAGNETIC-RESONANCE INVESTIGATIONS

ALIEV, AE; HARRIS, KDM; TEGZE, M; PEKKER, S; (1993) STRUCTURAL AND DYNAMIC PROPERTIES OF THE C-60/N-PENTANE INCLUSION COMPOUND - SOLID-STATE C-13 NUCLEAR-MAGNETIC-RESONANCE INVESTIGATIONS. J MATER CHEM , 3 (11) 1091 - 1094.

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Abstract

Variable-temperature solid-state C-13 NMR studies of the C60/n-pentane inclusion compound are reported, aimed towards understanding the structural and dynamic consequences of a low-temperature phase transition in this material. The phase transition occurs over a wide temperature range, between ca. 210 and 173 K. In the high-temperature phase, the two ends of the n-pentane molecule exchange rapidly (on the C-13 NMR timescale) between two crystallographically inequivalent end-group environments, whereas, in the low-temperature phase, this exchange process does not occur (on the C-13 NMR timescale).

Type: Article
Title: STRUCTURAL AND DYNAMIC PROPERTIES OF THE C-60/N-PENTANE INCLUSION COMPOUND - SOLID-STATE C-13 NUCLEAR-MAGNETIC-RESONANCE INVESTIGATIONS
Keywords: INCLUSION COMPOUND, BUCKMINSTERFULLERENE, SOLID-STATE NMR, NMR-SPECTRA, C60
UCL classification: UCL > School of BEAMS > Faculty of Maths and Physical Sciences > Chemistry
URI: http://discovery.ucl.ac.uk/id/eprint/139623
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