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Supercycled homonuclear dipolar decoupling sequences in solid-state NMR

Paul, S; Thakur, RS; Goswami, M; Sauerwein, AC; Mamone, S; Concistre, M; Forster, H; ... Madhu, PK; + view all (2009) Supercycled homonuclear dipolar decoupling sequences in solid-state NMR. J MAGN RESON , 197 (1) 14 - 19. 10.1016/j.jmr.2008.11.011.

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Abstract

We compare the performance of the windowed phase-modulated Lee-Goldburg (wPMLG) and the windowed decoupling using mind boggling optimisation (wDUMBO) sequences at various magic-angle spinning rates and nutation frequencies of the pulses. Additionally, we introduce a supercycled version of wDUMBO and compare its efficiency with that of the non-supercycled implementation of wDUMBO. The efficiency of the supercycled version of wPMLG, denoted wPMLG-S2, is compared with a new supercycled version of wPMLG that we notate as wPMLC-S3. The interaction between the supercycled homonuclear dipolar decoupling sequences and the sample rotation is analysed using symmetry-based selection rules. (C) 2008 Elsevier Inc. All rights reserved.

Type: Article
Title: Supercycled homonuclear dipolar decoupling sequences in solid-state NMR
DOI: 10.1016/j.jmr.2008.11.011
Keywords: Solid-state NMR, Homonuclear dipolar decoupling, PMLG, DUMBO, MAS, H-1 spectra, NUCLEAR-MAGNETIC-RESONANCE, HIGH-RESOLUTION H-1-NMR, MAGIC-ANGLE, MULTIPLE-PULSE, PROTON SPECTROSCOPY, SPINNING SOLIDS, HIGH-ORDER
UCL classification: UCL > Provost and Vice Provost Offices
UCL > Provost and Vice Provost Offices > School of Life and Medical Sciences
UCL > Provost and Vice Provost Offices > School of Life and Medical Sciences > Faculty of Life Sciences
UCL > Provost and Vice Provost Offices > School of Life and Medical Sciences > Faculty of Life Sciences > Div of Biosciences
UCL > Provost and Vice Provost Offices > School of Life and Medical Sciences > Faculty of Life Sciences > Div of Biosciences > Structural and Molecular Biology
URI: http://discovery.ucl.ac.uk/id/eprint/1325338
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