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A continuous and clean one-step synthesis of nano-particulate Ce(1- x)Zr(x)O<inf>2</inf> solid solutions in near-critical water

Cabanas, A; Darr, JA; Lester, E; Poliakoff, M; (2000) A continuous and clean one-step synthesis of nano-particulate Ce(1- x)Zr(x)O<inf>2</inf> solid solutions in near-critical water. Chemical Communications (11) pp. 901-902.

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Abstract

Gram-scale quantities of microcrystalline powdered CeO 2 -ZrO 2 solid solutions can be produced continuously in a near-critical water flow reactor at ca. 300 °C and 25 MPa; rapid hydrothermal co-precipitation leads to nano- particulate Ce(1-x)Zr(x)O(2) (x = 0 to 1), the composition of which is merely determined by the initial concentrations of Ce 4+ and Zr 4+ ions in the starting solution.

Type: Article
Title: A continuous and clean one-step synthesis of nano-particulate Ce(1- x)Zr(x)O<inf>2</inf> solid solutions in near-critical water
UCL classification: UCL > School of BEAMS
UCL > School of BEAMS > Faculty of Maths and Physical Sciences
URI: http://discovery.ucl.ac.uk/id/eprint/1323864
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