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Tracking the formation of cobalt substituted ALPO-5 using simultaneous in situ X-ray diffraction and X-ray absorption spectroscopy techniques

Simmance, K; Sankar, G; Bell, RG; Prestipino, C; van Beek, W; (2010) Tracking the formation of cobalt substituted ALPO-5 using simultaneous in situ X-ray diffraction and X-ray absorption spectroscopy techniques. PHYS CHEM CHEM PHYS , 12 (3) 559 - 562. 10.1039/b920245e.

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Abstract

We followed the formation of metal ion substituted aluminophosphate, a redox molecular sieve, using a newly developed in situ simultaneous X-ray diffraction and X-ray absorption spectroscopic technique. The study showed that a cobalt-phosphorous network forms prior to the crystallisation.

Type: Article
Title: Tracking the formation of cobalt substituted ALPO-5 using simultaneous in situ X-ray diffraction and X-ray absorption spectroscopy techniques
DOI: 10.1039/b920245e
Keywords: HYDROTHERMAL SYNTHESIS, POWDER DIFFRACTION, CRYSTALLIZATION, ZEOLITES, CATALYST, TIME, ALUMINOPHOSPHATES, MECHANISM, COAPO-5, XRD
UCL classification: UCL > School of BEAMS > Faculty of Maths and Physical Sciences
UCL > School of BEAMS > Faculty of Maths and Physical Sciences > Chemistry
URI: http://discovery.ucl.ac.uk/id/eprint/131534
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